Structures by: Portilla J.

Total: 82

2-(4-(4-Methoxyphenyl)-3-methyl-1-phenylindeno[1,2-b]pyrazolo[4,3-e]pyridin-5(1H)-ylidene)malononitrile'

C30H19N5O

Orrego-Hernández, JessicaLizarazo, CarolinaCobo, JustoPortilla, Jaime

RSC Advances (2019) 9, 47 27318

a=14.878(7)Å   b=12.149(6)Å   c=27.262(12)Å

α=90°   β=96.052(12)°   γ=90°

7-(4-Chlorophenyl)-3-iodo-2-methylpyrazolo[1,5-a]pyrimidine

C13H9ClIN3

Castillo, Juan-CarlosRosero, Hernán-AlejandroPortilla, Jaime

RSC Adv. (2017) 7, 45 28483

a=8.1315(6)Å   b=12.4851(8)Å   c=14.5014(7)Å

α=105.748(5)°   β=105.605(6)°   γ=99.832(6)°

1,3,5-tris(2-(tert-Butyl)pyrazolo[1,5-a]pyrimidin-7-yl)benzene

C150H162N36

Castillo, Juan-CarlosRosero, Hernán-AlejandroPortilla, Jaime

RSC Adv. (2017) 7, 45 28483

a=14.6829(3)Å   b=14.6829(3)Å   c=57.9972(11)Å

α=90°   β=90°   γ=120°

4-(4-Chlorophenyl)-2-methyl-1<i>H</i>-imidazole hemihydrate

C10H9Cl1N2,0.5(H2O1)

Macías, Mario A.Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 11

a=10.4027(15)Å   b=18.093(2)Å   c=11.1496(16)Å

α=90°   β=101.573(14)°   γ=90°

2-Methyl-4-phenyl-1<i>H</i>-imidazole

C10H10N2

Macías, Mario A.Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 11

a=29.196(4)Å   b=29.196(4)Å   c=5.4212(10)Å

α=90°   β=90°   γ=120°

4-(4-Methoxyphenyl)-2-methyl-1<i>H</i>-imidazole

C11H12N2O

Macías, Mario A.Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 11

a=7.1530(11)Å   b=7.4824(14)Å   c=21.437(3)Å

α=90°   β=90°   γ=90°

(<i>E</i>)-1-<i>tert</i>-Butyl-5-[(2,4-dichlorobenzylidene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H15Cl2N3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=6.5428(7)Å   b=7.9586(11)Å   c=30.415(5)Å

α=90°   β=92.987(13)°   γ=90°

(<i>E</i>)-1-<i>tert</i>-butyl-5-[(4-chlorobenzylidene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H16ClN3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.8317(14)Å   b=24.261(3)Å   c=6.9706(14)Å

α=90°   β=90°   γ=90°

(<i>E</i>)-1-<i>tert</i>-Butyl-5-[(pyridin-4-ylmethylene)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C15H16N4

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.1494(8)Å   b=9.0629(10)Å   c=9.4859(9)Å

α=92.465(8)°   β=97.113(8)°   γ=97.136(9)°

1-<i>tert</i>-Butyl-5-[(2,4-dichlorobenzyl)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H17Cl2N3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.9700(12)Å   b=9.3244(12)Å   c=10.4645(14)Å

α=105.057(12)°   β=103.589(12)°   γ=95.078(11)°

1-<i>tert</i>-Butyl-5-[(4-chlorobenzyl)amino]-1<i>H</i>-pyrrole-3-carbonitrile

C16H18ClN3

Macías, Mario A.Castillo, Juan-CarlosPortilla, Jaime

Acta Crystallographica Section C (2018) 74, 1 82-93

a=8.2422(10)Å   b=9.2361(10)Å   c=20.623(2)Å

α=90°   β=98.521(11)°   γ=90°

C18H14Cl2N2O

C18H14Cl2N2O

Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaMacías, Mario A.Portilla, Jaime

Acta Crystallographica Section B (2019) 75, 6

a=11.351(3)Å   b=16.259(6)Å   c=9.589(3)Å

α=90°   β=107.41(3)°   γ=90°

C18H14F2N2O

C18H14F2N2O

Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaMacías, Mario A.Portilla, Jaime

Acta Crystallographica Section B (2019) 75, 6

a=11.984(3)Å   b=9.537(2)Å   c=26.808(7)Å

α=90°   β=90°   γ=90°

C18H12Cl4N2O

C18H12Cl4N2O

Elejalde, Nerith-RocioButassi, EstefaníaZacchino, SusanaMacías, Mario A.Portilla, Jaime

Acta Crystallographica Section B (2019) 75, 6

a=4.4932(5)Å   b=10.9707(11)Å   c=18.786(2)Å

α=76.483(9)°   β=83.305(9)°   γ=78.976(9)°

8-methyl-7-(4-chlorophenyl)-10-phenyl-6,10-dihydro- 5H-benzo[h]pyrazolo[3,4-b]quinoline

C27H20ClN3

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=12.1072(4)Å   b=14.2672(5)Å   c=12.7635(4)Å

α=90.00°   β=109.953(8)°   γ=90.00°

8-methyl-7-(3-pyridinyl)-10-phenyl-6,10- dihydro-5H-benzo[h]pyrazolo[3,4-b]quinoline

C26H20N4

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=11.2274(6)Å   b=13.7079(8)Å   c=12.6935(7)Å

α=90.00°   β=95.731(3)°   γ=90.00°

11-(3,4,5-trimethoxyphenyl)-10-methyl-8-phenyl-6,8- dihydro-5H-benzo[f]pyrazolo[3,4-b]quinoline

C30H27N3O3

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=10.4716(9)Å   b=20.0027(18)Å   c=12.1529(9)Å

α=90.00°   β=107.818(4)°   γ=90.00°

8-methyl-7-(4-pyridinyl)-10-phenyl-10H- benzo[h]pyrazolo[3,4-b]quinoline

C26H18N4

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=11.3560(3)Å   b=17.3507(5)Å   c=9.7577(2)Å

α=90.00°   β=97.262(2)°   γ=90.00°

11-(4-methoxyphenyl)-10-methyl-8-phenyl-6,8-dihydro- 5H-benzo[f]pyrazolo[3,4-b]quinoline

C28H23N3O

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=18.0854(3)Å   b=21.2296(5)Å   c=23.8007(5)Å

α=90.00°   β=108.2580(10)°   γ=90.00°

11-(4-methylphenyl)-10-methyl-8-phenyl-6,8-dihydro- 5H-benzo[f]pyrazolo[3,4-b]quinoline

C28H23N3

Portilla, JaimeQuiroga, JairoNogueras, Manuelde la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section B (2008) 64, 1 72-83

a=11.1334(3)Å   b=11.4672(2)Å   c=17.6270(4)Å

α=97.858(2)°   β=106.135(3)°   γ=97.496(2)°

5-Butylamino-3-methyl-1-(pyridin-2-yl)-1<i>H</i>-pyrazole-4-carbaldehyde

C14H18N4O

Macías, Mario A.Orrego-Hernández, JessicaPortilla, Jaime

Acta Crystallographica Section E (2016) 72, 11 1672-1674

a=9.2854(2)Å   b=7.59144(18)Å   c=19.4452(5)Å

α=90°   β=102.818(3)°   γ=90°

Bis-(5-amino-3-methyl-1-phenyl-1H-pyrazol-4-yl)-3,4,5-trimethoxyphenylmethane

C30H32N6O3

Low, John N.Cobo, JustoPortilla, JaimeQuiroga, JairoGlidewell, Christopher

Acta Crystallographica Section E (2004) 60, 6 o1034-o1037

a=9.7540(2)Å   b=33.4646(7)Å   c=8.90100(10)Å

α=90.00°   β=103.6020(9)°   γ=90.00°

3,5-Dimethyl-1,7-diphenyl-1,7-dihydrodipyrazolo[3,4-b,4',3'-e]pyridine

C21H17N5

Portilla, Jaimede la Torre, Jose M.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section E (2006) 62, 5 o1676-o1678

a=21.2976(4)Å   b=10.9267(3)Å   c=7.4201(2)Å

α=90.00°   β=98.108(2)°   γ=90.00°

3,5-Dimethyl-1,7-diphenyl-4-(2-pyridinyl)-1H,7H-pyrazolo[3,4-b:4',3'-e]pyridine

C26H20N6

Low, John NicolsonCobo, JustoPortilla, JaimeQuiroga, Jairo

Acta Crystallographica Section E (2003) 59, 9 o1327-o1329

a=8.4576(2)Å   b=10.6599(3)Å   c=12.3642(4)Å

α=106.9170(14)°   β=98.6240(16)°   γ=100.803(2)°

3,5-Dimethyl-1,4,7-triphenyl-1H,7H-pyrazolo[3,4-b:4',3'-e]pyridine

C27H21N5

Low, John NicolsonCobo, JustoPortilla, JaimeQuiroga, Jairo

Acta Crystallographica Section E (2003) 59, 9 o1330-o1331

a=8.5006(2)Å   b=10.5829(3)Å   c=12.4093(3)Å

α=106.0775(12)°   β=97.6152(15)°   γ=100.6751(10)°

1-(p-Chlorophenyl)-3,4-dimethyl-5,6,7,8-tetrahydropyrazolo[3,4-b]quinoline

C18H18ClN3

Low, John NicolsonQuiroga, JairoPortilla, JaimeCobo, Justo

Acta Crystallographica Section E (2003) 59, 11 o1657-o1658

a=10.2097(6)Å   b=7.5773(3)Å   c=20.6921(12)Å

α=90.00°   β=110.203(3)°   γ=90.00°

6-(2-Hydroxybenzoyl)-2-(4-methylphenyl)-5-methyl-7- phenylpyrazolo[1,5-a]pyrimidine

C27H21N3O2

Portilla, JaimeTorre, José M. de laCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section E (2006) 62, 8 o3195-o3197

a=38.7649(11)Å   b=6.7864(2)Å   c=16.7002(5)Å

α=90.00°   β=108.599(2)°   γ=90.00°

8-tert-Butyl-7,10-diphenyl-6,10-dihydro-5H-benzo[h]pyrazolo[3,4-b]quinoline

C30H27N3

Low, John N.Cobo, JustoPortilla, JaimeQuiroga, JairoGlidewell, Christopher

Acta Crystallographica Section E (2007) 63, 5 o2690-o2691

a=9.516(2)Å   b=10.406(3)Å   c=11.868(5)Å

α=99.52(4)°   β=100.42(2)°   γ=91.55(4)°

N,N'-Bis(isonicotinoyl)hydrazine dihydrate

C12H10N4O2,2H2O

Quiroga, JairoPortilla, JaimeCobo, JustoTorre, José M. de laLow, John N.Glidewell, Christopher

Acta Crystallographica Section E (2007) 63, 4 o1687-o1690

a=28.1492(15)Å   b=24.1628(13)Å   c=3.7181(5)Å

α=90.00°   β=90.00°   γ=90.00°

5-Cyclohexylamino-3-methyl-1-(pyridin-2-yl)-1<i>H</i>-pyrazole-4-carbaldehyde

C16H20N4O

Orrego Hernandez, JessicaPortilla, JaimeCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 5

a=21.369(2)Å   b=20.489(3)Å   c=6.7444(10)Å

α=90°   β=95.978(10)°   γ=90°

(<i>Z</i>)-4-[(Cyclohexylamino)methylidene]-3-methyl-1-phenyl-1<i>H</i>-pyrazol-5(4<i>H</i>)-one

C17H21N3O

Orrego Hernandez, JessicaPortilla, JaimeCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2015) 71, 5

a=7.3348(3)Å   b=7.3614(10)Å   c=29.2335(6)Å

α=91.243(3)°   β=92.678(10)°   γ=101.004(4)°

10-methyl-8-phenyl-11-(3-pyridyl)-6,8-dihydro-5H- benzo[f]pyrazolo[3,4-b]quinoline

C26H20N4

Portilla, JaimeSerrano, HugoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o490-o492

a=19.2181(6)Å   b=19.2181(6)Å   c=10.8347(2)Å

α=90.00°   β=90.00°   γ=90.00°

10-methyl-8-phenyl-11-(4-pyridyl)-6,8-dihydro-5H- benzo[f]pyrazolo[3,4-b]quinoline

C26H20N4

Portilla, JaimeSerrano, HugoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o490-o492

a=18.6288(8)Å   b=19.1956(8)Å   c=10.8885(3)Å

α=90.00°   β=90.00°   γ=90.00°

5-methyl-2-(4-methylphenyl)-7,8-dihydro-6H- cyclopenta[g]pyrazolo[1,5-a]pyrimidine

C17H17N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 7 o452-o456

a=13.2882(7)Å   b=6.8383(4)Å   c=15.1947(8)Å

α=90.00°   β=104.018(3)°   γ=90.00°

2-(4-chlorophenyl)-5-methyl-7,8-dihydro-6H- cyclopenta[g]pyrazolo[1,5-a]pyrimidine

C16H14ClN3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 7 o452-o456

a=13.6800(11)Å   b=6.6669(6)Å   c=15.2010(16)Å

α=90.00°   β=106.980(6)°   γ=90.00°

(4-methoxyphenyl)-5-methyl- 7,8-dihydro-6H-cyclopenta[g]pyrazolo[1,5-a]pyrimidine

C17H17N3O

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 7 o452-o456

a=9.4691(3)Å   b=8.1711(2)Å   c=18.0278(6)Å

α=90.00°   β=95.3430(14)°   γ=90.00°

8-methyl-10-phenyl-6,10-dihydro-5H-benzo[h]pyrazolo[3,4-b]quinoline

C21H17N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o483-o489

a=7.0870(2)Å   b=10.1321(4)Å   c=11.7977(5)Å

α=87.501(2)°   β=73.171(3)°   γ=74.828(2)°

8-methyl-7,10-diphenyl-6,10-dihydro-5H-benzo[h]pyrazolo[3,4-b]quinoline

C27H21N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o483-o489

a=11.5561(4)Å   b=17.6751(7)Å   c=9.8469(3)Å

α=90.00°   β=98.599(2)°   γ=90.00°

8-methyl-7-(4-methylphenyl)-10-phenyl-6,10-dihydro-5H- benzo[h]pyrazolo[3,4-b]quinoline

C28H23N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o483-o489

a=12.0313(3)Å   b=14.3347(4)Å   c=12.7956(3)Å

α=90.00°   β=109.3092(14)°   γ=90.00°

7-(4-methoxyphenyl)-8-methyl-10-phenyl-6,10-dihydro-5H- benzo[h]pyrazolo[3,4-b]quinoline

C28H23N3O

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 8 o483-o489

a=12.9148(3)Å   b=17.5938(5)Å   c=9.8192(2)Å

α=90.00°   β=104.3370(17)°   γ=90.00°

2-(4-bromophenyl)-5-methyl-7,8-dihydro-6H- cyclopenta[g]pyrazolo[1,5-a]pyrimidine

C16H14BrN3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 7 o452-o456

a=13.5387(6)Å   b=6.8551(2)Å   c=15.2767(7)Å

α=90.00°   β=105.708(2)°   γ=90.00°

(3<i>Z</i>)-3-{1-[(5-phenyl-1<i>H</i>-pyrazol-3-yl)amino]ethylidene}-4,5- dihydrofuran-2(3<i>H</i>)-one

C15H15N3O2

Quiroga, JairoPortilla, JaimeCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 1 o25-o28

a=10.4969(17)Å   b=9.8550(9)Å   c=12.6739(16)Å

α=90.00°   β=99.883(9)°   γ=90.00°

(3<i>Z</i>)-3-{1-[(5-methyl-1<i>H</i>-pyrazol-3-yl)amino]ethylidene}-4,5- dihydrofuran-2(3<i>H</i>)-one--6-(2-hydroxyethyl)-2,5- dimethylpyrazolo[1,5-<i>a</i>]pyrimidin-7(4<i>H</i>)-one (1/1)

C10H13N3O2,C10H13N3O2

Quiroga, JairoPortilla, JaimeCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 1 o25-o28

a=8.0402(11)Å   b=8.2025(17)Å   c=15.348(3)Å

α=91.999(14)°   β=99.785(12)°   γ=99.172(15)°

7-Amino-2,5-dimethylpyrazolo[1,5-a]pyrimidine hemihydrate

C8H10N4,0.5H2O

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 4 o186-o189

a=16.0851(5)Å   b=7.9458(3)Å   c=8.0003(3)Å

α=90.00°   β=117.309(2)°   γ=90.00°

3-(3-Oxo-1,3-dihydroisobenzofuran-1-ylidene)pentane-2,4-dione

C13H10O4

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 6 o332-o333

a=8.2779(3)Å   b=8.4719(6)Å   c=15.1413(12)Å

α=90.0°   β=95.534(6)°   γ=90.0°

8-<i>tert</i>-Butyl-7-(4-chlorophenyl)-10-phenyl-5,6-dihydro-10<i>H</i>- benzo[<i>h</i>]pyrazolo[3,4-<i>b</i>]quinoline

C30H26ClN3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 10 o582-o584

a=13.1170(18)Å   b=15.948(3)Å   c=17.717(2)Å

α=93.750(11)°   β=91.803(9)°   γ=101.155(13)°

7-Amino-5-methyl-2-phenyl-6-(phenyldiazenyl)pyrazolo[1,5-<i>a</i>]pyrimidine

C19H16N6

Portilla, JaimeEstupiñan, DiegoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 3 o133-o136

a=9.6342(13)Å   b=33.216(5)Å   c=9.747(3)Å

α=90.00°   β=90.237(18)°   γ=90.00°

9-(4-Chlorophenyl)-7-methyl-5,6-dihydrobenzo[h]pyrazolo[3,2-b]quinazoline

C21H16ClN3

Low, John N.Cobo, JustoQuiroga, JaimePortilla, JaimeGlidewell, Christopher

Acta Crystallographica Section C (2004) 60, 8 o604-o607

a=9.2382(8)Å   b=10.3054(8)Å   c=10.3184(9)Å

α=62.720(4)°   β=83.098(4)°   γ=70.531(5)°

2-(4-Chlorophenyl)-5-methyl-6,7-dihydrobenzo[e]pyrazolo[2,3-b]quinazoline

C21H16ClN3

Low, John N.Cobo, JustoQuiroga, JaimePortilla, JaimeGlidewell, Christopher

Acta Crystallographica Section C (2004) 60, 8 o604-o607

a=7.0098(3)Å   b=15.0306(7)Å   c=17.0060(8)Å

α=111.492(2)°   β=101.406(3)°   γ=97.981(3)°

5-Methyl-<i>N</i>-[2-nitro-4-(trifluoromethyl)phenyl]-1<i>H</i>-pyrazole- 3-amine

C11H9F3N4O2

Portilla, JaimeOntiveros, InaCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2013) 69, 2 172-174

a=4.957(2)Å   b=8.737(3)Å   c=13.562(5)Å

α=93.22(3)°   β=97.02(3)°   γ=91.05(3)°

5-Amino-1-benzoyl-3-methylpyrazole

C11H11N3O

Quiroga, JairoPortilla, JaimeHursthouse, Michael B.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2010) 66, 4 o159-o162

a=14.7443(6)Å   b=5.7669(2)Å   c=12.0082(3)Å

α=90.00°   β=106.119(2)°   γ=90.00°

Ethyl 4-(5-amino-3-methyl-1H-pyrazol-1-yl)benzoate

C13H15N3O2

Portilla, JaimeMata, Ernesto G.Nogueras, ManuelCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o21-o25

a=7.2228(4)Å   b=8.4433(3)Å   c=10.5938(5)Å

α=98.234(3)°   β=107.609(2)°   γ=97.907(3)°

4-(5-Amino-3-methyl-1H-pyrazol-1-yl)benzoic acid monohydrate

C11H11N3O2,H2O

Portilla, JaimeMata, Ernesto G.Nogueras, ManuelCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o21-o25

a=8.0166(2)Å   b=7.5082(2)Å   c=18.5507(5)Å

α=90.00°   β=91.8140(16)°   γ=90.00°

7-Amino-2-tert-butyl-5-methylpyrazolo[1,5-a]pyrimidine

C11H16N4

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o26-o28

a=10.8271(2)Å   b=10.8271(2)Å   c=19.9208(3)Å

α=90.00°   β=90.00°   γ=90.00°

Methyl 4-[(5-methyl-1H-pyrazol-3-yl)amino]-3-nitrobenzoate

C12H12N4O4

Portilla, JaimeMata, Ernesto G.Nogueras, ManuelCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o38-o41

a=5.9233(3)Å   b=8.8858(6)Å   c=11.7819(6)Å

α=85.690(4)°   β=83.500(4)°   γ=84.015(3)°

Methyl 1-(5-methyl-1H-pyrazol-3-yl)-1H-benzimidazole-5-carboxylate

C13H12N4O2

Portilla, JaimeMata, Ernesto G.Nogueras, ManuelCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o38-o41

a=8.3646(3)Å   b=11.5735(6)Å   c=12.7953(7)Å

α=88.328(3)°   β=88.526(3)°   γ=75.362(3)°

7-amino-5-tert-butyl-2-methylpyrazolo[1,5-a]pyrimidine

C11H16N4

Portilla, JaimeQuiroga, JairoTorre, José M. de laCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 8 o521-o524

a=9.8216(5)Å   b=11.3582(7)Å   c=12.2783(8)Å

α=70.429(3)°   β=69.895(4)°   γ=66.454(4)°

3,7-diamino-2,5-dimethylpyrazolo[1,5-a]pyrimidine monohydrate

C8H11N5,H2O

Portilla, JaimeQuiroga, JairoTorre, José M. de laCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2006) 62, 8 o521-o524

a=8.0970(2)Å   b=9.8881(3)Å   c=11.9661(3)Å

α=90.00°   β=96.230(5)°   γ=90.00°

2,5-Dimethyl-6,7-dihydrobenzo[h]pyrazolo[1,5-a]quinazoline

C16H15N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 8 o458-o461

a=7.9430(19)Å   b=7.9660(11)Å   c=9.943(3)Å

α=87.637(13)°   β=82.632(18)°   γ=89.941(17)°

2-tert-Butyl-5-methyl-6,7-dihydrobenzo[h]pyrazolo[1,5-a]quinazoline

C19H21N3

Portilla, JaimeQuiroga, JairoCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 8 o458-o461

a=11.2632(5)Å   b=11.4574(7)Å   c=12.1317(6)Å

α=93.449(5)°   β=90.313(4)°   γ=102.791(6)°

Methyl 4-(5-amino-3-phenyl-1<i>H</i>-pyrazol-1-yl)-3-nitrobenzoate

C17H14N4O4

Portilla, JaimeMata, Ernesto G.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 9 o510-o513

a=12.3516(8)Å   b=7.5202(4)Å   c=17.1564(13)Å

α=90.00°   β=100.699(5)°   γ=90.00°

Methyl 3-nitro-4-[(5-phenyl-1<i>H</i>-pyrazol-3-yl)amino]benzoate

C17H14N4O4

Portilla, JaimeMata, Ernesto G.Cobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 9 o510-o513

a=31.0506(4)Å   b=5.4210(11)Å   c=20.7251(12)Å

α=90.00°   β=121.071(6)°   γ=90.00°

5-Amino-1-(4-methoxybenzoyl)-3-methylpyrazole

C12H13N3O2

Quiroga, JairoPortilla, JaimeLow, John N.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2008) 64, 2 o76-o79

a=6.1920(15)Å   b=9.192(2)Å   c=10.546(2)Å

α=73.69(2)°   β=85.634(17)°   γ=82.83(3)°

5-Amino-3-methyl-1-(2-nitrobenzoyl)pyrazole

C11H10N4O3

Quiroga, JairoPortilla, JaimeLow, John N.Cobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2008) 64, 2 o76-o79

a=11.4212(15)Å   b=7.1787(14)Å   c=13.2595(10)Å

α=90.00°   β=90.00°   γ=90.00°

5-methyl-2-phenyl-6,7-dihydrobenzo[h]pyrazolo[1,5-a]quinazoline

C21H17N3

Portilla, JaimeQuiroga, JairoCobo, JustoNogueras, ManuelLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 6 o398-o403

a=7.6223(2)Å   b=16.7937(7)Å   c=24.4900(9)Å

α=90.00°   β=90.00°   γ=90.00°

5-methyl-2-(4-methylphenyl)-6,7-dihydrobenzo[h]pyrazolo[1,5-a]quinazoline

C22H19N3

Portilla, JaimeQuiroga, JairoCobo, JustoNogueras, ManuelLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 6 o398-o403

a=7.2767(13)Å   b=29.924(6)Å   c=8.0463(12)Å

α=90.00°   β=112.590(6)°   γ=90.00°

7-methyl-10-phenyl-5,6-dihydrobenzo[h]pyrazolo[5,1-b]quinazoline

C21H17N3

Portilla, JaimeQuiroga, JairoCobo, JustoNogueras, ManuelLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 6 o398-o403

a=8.10920(10)Å   b=11.7265(2)Å   c=16.3486(3)Å

α=90.00°   β=90.9010(12)°   γ=90.00°

7-methyl-10-(4-methylphenyl)-5,6-dihydrobenzo[h]pyrazolo[5,1-b]quinazoline

C22H19N3

Portilla, JaimeQuiroga, JairoCobo, JustoNogueras, ManuelLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2005) 61, 6 o398-o403

a=7.9037(7)Å   b=13.1038(10)Å   c=16.0576(13)Å

α=90.00°   β=99.199(6)°   γ=90.00°

2-<i>tert</i>-Butyl-5-methyl-7,8-dihydro-6<i>H</i>- cyclopenta[<i>e</i>]pyrazolo[1,5-<i>a</i>]pyrimidine

C14H19N3

Portilla, JaimeQuiroga, JairoCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2008) 64, 9 o471-o473

a=6.8665(6)Å   b=9.4084(14)Å   c=11.147(2)Å

α=91.611(14)°   β=107.728(14)°   γ=111.097(12)°

3-<i>tert</i>-butyl-1-(4-chlorophenyl)-4- phenylindeno[1,2-<i>b</i>]pyrazolo[4,3-<i>e</i>]pyridin-5(1<i>H</i>)-one

C29H22ClN3O

Portilla, JaimeLizarazo, CarolinaCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2011) 67, 12 o479-o483

a=8.1014(5)Å   b=11.3554(10)Å   c=13.5762(11)Å

α=102.755(7)°   β=90.013(8)°   γ=108.268(7)°

3-<i>tert</i>-butyl-1-(4-chlorophenyl)-4- (4-methoxyphenyl)indeno[1,2-<i>b</i>]pyrazolo[4,3-<i>e</i>]pyridin-\ 5(1<i>H</i>)-one

C30H24ClN3O2

Portilla, JaimeLizarazo, CarolinaCobo, JustoGlidewell, Christopher

Acta Crystallographica Section C (2011) 67, 12 o479-o483

a=11.1911(9)Å   b=11.4258(8)Å   c=20.095(2)Å

α=97.411(6)°   β=93.272(7)°   γ=107.635(6)°

C72H60Cu4I4P4[solvent]

C72H60Cu4I4P4[solvent]

Castillo, Juan-CarlosBravo, Nestor-FabianTamayo, Lenka-VictoriaMestizo, Paula-DanielaHurtado, JohnMacías, MarioPortilla, Jaime

ACS omega (2020) 5, 46 30148-30159

a=18.3661(16)Å   b=16.0719(14)Å   c=27.117(3)Å

α=90°   β=108.602(10)°   γ=90°

C29H31CuIN4P

C29H31CuIN4P

Castillo, Juan-CarlosBravo, Nestor-FabianTamayo, Lenka-VictoriaMestizo, Paula-DanielaHurtado, JohnMacías, MarioPortilla, Jaime

ACS omega (2020) 5, 46 30148-30159

a=10.7747(8)Å   b=15.4475(10)Å   c=19.6421(12)Å

α=109.743(6)°   β=99.759(5)°   γ=103.575(6)°

C13H12N4O2

C13H12N4O2

Orrego-Hernández, JessicaPortilla, Jaime

The Journal of organic chemistry (2017) 82, 24 13376-13385

a=11.29659(18)Å   b=28.0997(4)Å   c=7.63435(10)Å

α=90°   β=96.3340(13)°   γ=90°

C14H11N3O

C14H11N3O

Castillo, Juan-CarlosTigreros, AlexisPortilla, Jaime

The Journal of organic chemistry (2018) 83, 18 10887-10897

a=14.466(2)Å   b=7.8330(15)Å   c=20.727(4)Å

α=90°   β=98.549(15)°   γ=90°

C23H21N3O4

C23H21N3O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=10.0379(13)Å   b=10.2812(13)Å   c=10.6299(13)Å

α=73.378(11)°   β=83.687(10)°   γ=80.048(11)°

C26H25ClN4O4

C26H25ClN4O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=7.0920(15)Å   b=34.990(8)Å   c=9.922(3)Å

α=90°   β=98.12(3)°   γ=90°

C26H25N4O4

C26H25N4O4

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=7.1294(7)Å   b=32.835(3)Å   c=10.2161(9)Å

α=90°   β=96.947(9)°   γ=90°

C23H18ClN3O3

C23H18ClN3O3

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=16.130(2)Å   b=17.057(3)Å   c=15.338(2)Å

α=90°   β=106.066(14)°   γ=90°

C28H20FN3O3,C3H7NO

C28H20FN3O3,C3H7NO

Charris-Molina, AndrésCastillo, Juan-CarlosMacías, MarioPortilla, Jaime

The Journal of organic chemistry (2017) 82, 23 12674-12681

a=10.8530(15)Å   b=12.0931(16)Å   c=12.7462(12)Å

α=111.386(10)°   β=93.203(10)°   γ=111.842(13)°

C10H9N3O

C10H9N3O

Castillo, Juan-CarlosEstupiñan, DiegoNogueras, ManuelCobo, JustoPortilla, Jaime

The Journal of organic chemistry (2016) 81, 24 12364-12373

a=6.8354(5)Å   b=11.3494(10)Å   c=12.1390(9)Å

α=90°   β=104.352(2)°   γ=90°

Methyl 4-(5-amino-3-tert-butyl-1H-pyrazol-1-yl)benzoate

C15H19N3O2

Portilla, JaimeMata, Ernesto G.Nogueras, ManuelCobo, JustoLow, John N.Glidewell, Christopher

Acta Crystallographica Section C (2007) 63, 1 o21-o25

a=6.1272(2)Å   b=11.6374(3)Å   c=20.3182(7)Å

α=90.00°   β=98.629(2)°   γ=90.00°